Automatic sampling differential scanning calorimeter

Type Differential scanning calorimeter
Usage Differential scanning calorimetry (DSC) is a classical thermal analysis method for thermal effects under controlled program temperature.
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Detail

■ Instrument use


Differential scanning calorimetry (DSC), as a classical thermal analysis method of thermal effect under controlled program temperature, has been widely used in the research and development, process optimization, quality control and failure analysis of various materials and chemistry fields. Using DSC, we can study the phase transformation of inorganic materials, melting of polymer materials, crystallization process, polycrystalline phenomenon of drugs, solid/liquid phase ratio of food such as fats and fats.


■ Instrument features


1. Equipped with 40 bit automatic sampler, smart volume, easy to place in the laboratory, unattended test operation, greatly saving labor costs and improving experimental efficiency.


2. Hot flow differential scanning calorimeter has good repeatability and high accuracy, especially suitable for accurate measurement of specific heat.


3. The whole machine integration, temperature control and furnace device into one, reduce signal loss and interference.


4. Perfect two-way atmosphere control system, using mass flow controller; During the measurement process, two air intake modes can be selected, and the software sets automatic switching.


5. The instrument is equipped with standard substances, and the user can correct each temperature segment by himself to reduce the error of the instrument.


6. Intelligent software design, automatic drawing of the instrument, software can realize a variety of data processing, such as enthalpy calculation, glass transition temperature, oxidation induction period, substance melting point and crystallization and so on.


7. The instrument can automatically generate DSC and oxidation induction period experiment report.


8. Large screen LCD display, real-time display of instrument status and data, two sets of temperature measurement couples, one set of couples to display the sample temperature at work, the other set of couples to display real-time furnace temperature (whether the heating furnace is working or not).


9. The machine is equipped with RS232 and USB interface and intelligent software, which can realize automatic program control and setting.


10. The instrument has the function of remote operation, maintenance and adjustment (the instrument can be remotely operated through the Internet).


■ Instrument index


Temperature data

DSC data

Temperature range

Room temperature up to 680 °C (different control methods can be selected, the lowest temperature can be minus 150°C)

Measuring range

±500mw

Minimum resolution

±0.1μw

Temperature accuracy

±0.1℃

Power noise

±0.1μw

Heating rate

0.1℃/min~100℃/min

Power accuracy

±0.1μw

Temperature resolution

±0.1℃

Thermostatic controller, thermostatic gas chromatography, mass spectrometry connector, thermostatic band

Constant temperature range: room temperature ~200°

Temperature control mode

Heating, constant temperature, cooling (program automatic control)

Display mode

Chinese characters large screen LCD display

Atmosphere system

Gas mass flow controller;Automatic switching between two gas channels can be set

Crucible volume

0.06mL

Gas velocity

0~200mL/min(other ranges can be customized)

Crucible arrangement

Aluminum oxide, high purity aluminum (standard)

Optional crucible

Sealing liquid aluminum crucible (with sealing device) Sealing solid aluminum crucible (with sealing device) Zirconia, quartz, graphite, platinum rhodium (users can choose according to their own needs)

Software advantage

Intelligent, selectable baseline correction with reference materials (indium, tin, lead, zinc, aluminum) allows users to adjust temperature and enthalpy on their own